HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → HCID 20467884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-Hydroxy-1-indanone | HCID 590547 | — |
| Reactant | HCID 12277192 | HCID 12277192 | — |
| Reactant | 1H-Indene-1,4-diol, 2,3-dihydro-, 4-acetate | HCID 12734709 | — |
| Product | HCID 20467884 | HCID 20467884 | — |
Reaction Steps
4-Hydroxy-1-indene is prepared starting from 4-hydroxyindanone via 1,4-indanediol, 4-acetoxy-1-indanol and 4-acetoxy-1-indene in this order. The resulting 4-hydroxy-1-indene is allowed to react with epichlorohydrin in an aqueous solution of sodium hydroxide to give 4-(2,3-epoxypropoxy)indene. [cf. Yakugaku Zasshi 92, 1358 (1972)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04435397 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-98de39b3a9b34b7d876ff60f4a9d45c6 |
| Source note | uspto-grants-1984_03 |