Methyl iodide → HCID 20468253, compound

HRID 1903136Notes

Reaction equation

HRID 1903136 reaction equation
[NH:1]1[CH2:6][CH2:5][CH2:4][CH:3]([C:7]2[CH:15]=[CH:14][CH:13]=[C:12]3[C:8]=2[CH2:9][C:10](=[O:16])[NH:11]3)[CH2:2]1.[CH3:17]I>>[CH3:17][N:1]1[CH2:6][CH2:5][CH2:4][CH:3]([C:7]2[CH:15]=[CH:14][CH:13]=[C:12]3[C:8]=2[CH2:9][C:10](=[O:16])[NH:11]3)[CH2:2]1

Participants

3

Procedure

Using the procedure of Example 3, 1,3-dihydro-4-(piperidin-3-yl)-2H-indole-2-one and methyl iodide were reacted to obtain 1,3-dihydro-4-(1-methyl-piperidin-3-yl)-2H-indole-2-one which melted at 160° C. after crystallization from benzene.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-7036348a656542e3b4948895de83b6dc
Source dataset
uspto-grants-1984_03
Patent number
US04435408

Reaction notes

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