Hydrochloric Acid → HCID 13274422, compound

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Reaction Steps

The compound of the title, as the free base, is prepared by following essentially the same procedure described in example 2 but using 7-methoxy-2-methylamino-1-nitrosonaphthalene instead of 2-methylamino-1-nitrosonaphthalene and 4-methoxybenzaldehyde instead of 4-ethoxybenzaldehyde. By addition of HCl to a diethyl ether solution of the free base, the corresponding hydrochloride precipitates. Yield 40%. M.p. 265° C. dec. (from methanol).

Provenance & Evidence