HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 20468233, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 13200302 | HCID 13200302 | — |
| Product | HCID 20468233 | HCID 20468233 | — |
Reaction Steps
3-(p-Carboxyphenyl)-2-(2-dimethylaminoethylthio)quinoline (0.7 g.) was added to a solution of thionyl chloride (1.5 ml.) in methanol (20 ml.) at 0°. The mixture was stirred at ambient temperature for 16 hr., and the solvent then evaporated. The solid residue was crystallised from methanol-ethyl acetate to give 2-(2-dimethylaminoethylthio)-3-(p-methoxycarbonylphenyl)quinoline hydrochloride, m.p. 224-5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04435405 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-19050a81e94644429e3c746a0c6565e7 |
| Source note | uspto-grants-1984_03 |