HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-Ethyl-3-phenylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 178464749 | HCID 178464749 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-Ethyl-3-phenylurea | HCID 12115 | 79% |
Reaction Steps
5.08 g ethylcarbamoyl-benzoic acid sulfimide was reacted with 1.86 g aniline and 2.8 ml triethylamine in 20 ml of a 1:1 mixture of water and acetone, as described in example 1. 2.59 g 1-phenyl-3-ethylurea was obtained, melting at 99°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04435567 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-35440c9b9e2543be8db34146e9f698d2 |
| Source note | uspto-grants-1984_03 |