HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dodecanal → Tert-butyl 3-hydroxytetradecanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dodecanal | HCID 8194 | — |
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | Tert-butyl 3-hydroxytetradecanoate | HCID 14247856 | 80.7% |
Reaction Steps
The reaction of dodecanal (0.92 g) and tert-butyl bromoacetate (1.56 g) was carried out under the presence of zinc (0.59 g) according to similar manner to that of Preparation 1-(1) to afford an oil of tert-butyl 3-hydroxytetradecanoate (1.21 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04436726 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-483640d3b9a64d0e9e025bf81d86a151 |
| Source note | uspto-grants-1984_03 |