HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexanal → Tert-butyl 3-hydroxyoctanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexanal | HCID 6184 | — |
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | Tert-butyl 3-hydroxyoctanoate | HCID 20467271 | 77.2% |
Reaction Steps
The reaction of hexanal (720 mg) and tert-butyl bromoacetate (2.265 g) was carried out under the presence of zinc (850 mg) according to similar manner to that of Preparation 1-(1) to afford an oil of tert-butyl 3-hydroxyoctanoate (1.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04436726 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-5cdba11fa8984890ad8d24d9ed81c983 |
| Source note | uspto-grants-1984_03 |