HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethyl-1,3-dioxane-4,6-dione → 5-(1-Hydroxy-9-octadecenylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
| Reactant | 9-Octadecenoyl chloride | HCID 66987 | — |
| Product | 5-(1-Hydroxy-9-octadecenylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione | HCID 70446691 | 88.4% |
Reaction Steps
Starting from 9-octadecenoyl chloride (15 g) and 2,2-dimethyl-1,3-dioxane-4,6-dione (8 g), 5-(1-hydroxy-9-octadecenylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione (18 g) was obtained as oil according to a similar manner to that of Preparation A-2(1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04436726 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-f65db66665ba4b799f317cd306615cd2 |
| Source note | uspto-grants-1984_03 |