HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-phenyl-2-naphthylamine → HCID 57232163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-phenyl-2-naphthylamine | HCID 8679 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzene, 1-iodo-3-methoxy- | HCID 69839 | — |
| Catalyst | Copper | HCID 23978 | — |
| Solvent | Nitrobenzene | HCID 7416 | — |
| Product | HCID 57232163 | HCID 57232163 | 67.3% |
Reaction Steps
A mixture of 43.8 g (0.2 mol) of phenyl-β-naphthylamine, 46.8 g (0.2 mol) of m-iodoanisol, 27.6 g (0.2 mol) of anhydrous potassium carbonate, 2 g of copper powder and 300 ml of nitrobenzene was heated under reflux for 15 hours. The inorganic substances were filtered off and the nitrobenzene was distilled off. The residue obtained was then processed by column chromatography to obtain 43.8 g of phenyl-β-naphthyl-3-methoxyphenylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04436920 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-ddd48cbc0be34e20a7fdbda30a4f517c |
| Source note | uspto-grants-1984_03 |