HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(2-Phenylpropan-2-yl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Alpha-Methylstyrene | HCID 7407 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Product | 4-(2-Phenylpropan-2-yl)aniline | HCID 234874 | 78% |
Reaction Steps
18.6 Parts of aniline, 20.4 parts of 36% w/w hydrochloric acid containing 13.6 parts of zinc chloride are stirred and refluxed for 24 hours with 23.6 parts of α-methylstyrene. The work-up follows Example 3 and gives on distillation 32.9 parts of 4-cumylaniline mb4 175°-80° C. (78% yield based on a 93% purity by G.L.C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04436936 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-7b16dcf794b84a99b98182202059afda |
| Source note | uspto-grants-1984_03 |