HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 70502727, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 70503253 | HCID 70503253 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 70502727 | HCID 70502727 | — |
Reaction Steps
To 5.3 g of benzyloxycarbonyl-L-alanyl-2-(2,5-dioxopyrrolidin-3-yl)glycine benzhydryl ester was added 10 ml of a 30% solution of hydrogen bromide in acetic acid and the mixture was stirred at room temperature for one hour. To the reaction mixture was added ethyl ether and the resulting precipitate was collected by filtration. Yield 3.2 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04436918 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-d425794c41664fe08df1fc3d8fa55dc3 |
| Source note | uspto-grants-1984_03 |