HRID1903781

反应详情

EQUATION

反应方程式

HRID 1903781 的结构方程式

PROCEDURE

实验过程

4.15 g. 4-Propoxyphenyl glycidyl ether and 6.6 g. N-(2,6-dimethylphenyl)-ethylenediamine are left to stand for 3 days at ambient temperature and the reaction mixture then separated by ion exchange chromatography in the manner described in Example 5. There are obtained 4.3 g. (58% of theory) of the desired product in the form of colorless crystals; m.p. 51°-54° C. The corresponding neutral fumarate, after recrystallization from ethanol, melts at 168°-169° C.

WORKUP

后处理

  1. customthe reaction mixture then separated by ion exchange chromatography in the manner
  2. customThere are obtained 4.3 g