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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1903863Generated: November 1, 2026

Boc-Tyr-(D)Ala-Gly-Phe methioninol → H-Tyr-(D)Ala-Gly-Phe methioninol

https://huagongshe.com/reaction/1903863

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBoc-Tyr-(D)Ala-Gly-Phe methioninolHCID 131712172—
SolventTrifluoroacetic acid methylene chlorideHCID 21863450—
ProductH-Tyr-(D)Ala-Gly-Phe methioninolHCID 131712171—

Reaction Steps

2.0 g of Boc-Tyr-(D)Ala-Gly-Phe-methioninol are dissolved in 20 ml of TFA--CH2Cl2 (1:1) and left to stand for 30 minutes at 0°. After reducing the volume under vacuum, the title compound is precipitated with ether and filtered off. The title compound is obtained as an amorphous salt.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04438103
Source datasetuspto-grants-1984_03
ORD IDord-644856202d9a4e37b77179e1eed1d5b8
Source noteuspto-grants-1984_03