HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl orthoacetate → HCID 13290541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl orthoacetate | HCID 66221 | — |
| Reactant | HCID 20456649 | HCID 20456649 | — |
| Product | HCID 13290541 | HCID 13290541 | — |
Reaction Steps
A solution of 7 g of 6B in 50 ml of triethyl orthoacetate was heated at 140° C. for 2 hours. The resulting mixture was cooled to room temperature, absorbed on silica gel and chromatographed, using the eluent described in Example 1, to give 6, as a viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04439226 |
| Source dataset | uspto-grants-1984_03 |
| ORD ID | ord-49f08f0fa05e4107864dd1a836adf14b |
| Source note | uspto-grants-1984_03 |