Sodium Hydroxide → HCID 20465938, compound

Participants

Reaction Steps

To a solution of 2 g of 3-butanesulfonamido-N-[2-(5-dimethylaminomethylfuran-2-ylmethylthio)ethyl]benzamide oxalate in 10 ml of water there is added sodium hydroxide until a strong basic reaction is obtained. The mixture is extracted with a mixture ethyl acetate:ethanol 9:1, the organic phase is dried over anhydrous sodium sulfate and evaporated to dryness. Thus, there is obtained 1.5 g of 3-butanesulfonamido-N-[2-(5-dimethylaminomethylfuran-2-ylmethylthio)ethyl]benzamide as an oily yellowish product.

Provenance & Evidence