HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lauric Acid → Hexahydro-1-lauroyl-1H-azepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lauric Acid | HCID 3893 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Azepane | HCID 8119 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Hexahydro-1-lauroyl-1H-azepine | HCID 96224 | 83.5% |
Reaction Steps
A mixture of dodecanoic acid (20.03 g, 0.1M), acetic anhydride (13.27 g, 0.13M), hexahydro-1H-azepine (12.9 g, 0.13M) was heated with distillation of formed acetic acid. The residue on distillation gave 23.46 g (83.5%) of colorless product, b.p. 204-205/7 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837026 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-651a80f6587842b081a78181acadd43f |
| Source note | uspto-grants-1989_06 |