HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 14671834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-Chloro-2-(1,1-dimethylethyl)-5-mercapto-3(2H)-pyridazinone | HCID 13469242 | — |
| Reactant | HCID 14671833 | HCID 14671833 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14671834 | HCID 14671834 | 44.1% |
Reaction Steps
In 30 ml of 95% ethanol were dissolved 1.5 g of 2-t-butyl-4-chloro-5-mercapto-3(2H)-pyridazinone and 1.8 g of 4-(2-methoxy-1-methylethoxy)-benzyl bromide, and thereto was added 0.48 g of powdery potassium hydroxide. The reaction mixture was stirred overnight at room temperature. Then, similarly to the procedures in Preparation Example 3, there was obtained 1.2 g of the aimed product, m.p. 51.0°~52.0° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837217 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-f16698a4371b477586943a5da8580615 |
| Source note | uspto-grants-1989_06 |