HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1904412Generated: November 1, 2026
Triphenylphosphine → HCID 18000289, compound
https://huagongshe.com/reaction/1904412
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 23112134 | HCID 23112134 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18000289 | HCID 18000289 | — |
Reaction Steps
A mixture of 3-(bromoethyl)benzoic acid, ethyl ester (12.2 g, 0.050 mol) and triphenyl phosphine (13.1 g, 0.05 mol) in toluene (50 ml) was stirred at 70° C. for 16 hours to yield [[3-(ethoxycarbonyl)phenyl]methyl]triphenylphosphonium bromide as a colorless crystalline solid which was filtered off, washed with toluene and dried under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04837333 |
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| Source dataset | uspto-grants-1989_06 |
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| ORD ID | ord-281db3cf0a884595942153cdc889313d |
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| Source note | uspto-grants-1989_06 |
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