HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Ethyl Ketone → 4,4'-Dichlorobenzoin toluenesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Ethyl Ketone | HCID 6569 | — |
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | 1,2-Bis(4-chlorophenyl)-2-hydroxyethanone | HCID 219286 | — |
| Product | 4,4'-Dichlorobenzoin toluenesulfonate | HCID 86743111 | — |
Reaction Steps
In accordance with Example 2, p-toluenesulfonyl chloride is reacted with 4,4'-dichlorobenzoin in 200 ml of methyl ethyl ketone. The resultant sulfone melts at 129°-130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837350 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-e887490e16844619909c54cb96ba714c |
| Source note | uspto-grants-1989_06 |