HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → (Methyl)tri-4-tolylphosphonium Iodide-d3,13C
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Phosphine, tris(4-methylphenyl)- | HCID 13956 | — |
| Product | (Methyl)tri-4-tolylphosphonium Iodide-d3,13C | HCID 19438167 | 91.5% |
Reaction Steps
Starting from 10.37 g (34.1 mmol) of tris(4-methylphenyl)phosphine and 6.7 g (48 mmol, 1.4 eq) of methyl iodide, 13.92 g (31.2 mmol, 91.5%) of methyltris(4-methylphenyl)phosphonium iodide was obtained: mp 213°-216° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837392 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-c6ee8144b77949668ad0f52e3662ac7f |
| Source note | uspto-grants-1989_06 |