HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 2778290, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Phosphine, tris(4-methoxyphenyl)- | HCID 70071 | — |
| Product | HCID 2778290 | HCID 2778290 | 93.3% |
Reaction Steps
Starting from 10.4 g (29.5 mmol) of tris(4-methoxyphenyl)phosphine and 6.7 g (48 mmol, 1.6 eq) of methyl iodide, 13.6 g (27.5 mmol, 93.3%) of methyltris(4-methoxyphenyl)phosphonium iodide was obtained: mp 220.1°-221.9° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837392 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-d8a7d7f6e1a94cbfa432719722274adb |
| Source note | uspto-grants-1989_06 |