HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Tris(4-chlorophenyl)(methyl)phosphanium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Tris(4-chlorophenyl)phosphine | HCID 70874 | — |
| Product | Tris(4-chlorophenyl)(methyl)phosphanium iodide | HCID 2778284 | 92.9% |
Reaction Steps
Starting from 8.28 g (22.6 mmol) of tris(4-chlorophenyl)phosphine and 5.7 g (40 mmol, 1.8 eq) of methyl iodide, 10.64 g (21.0 mmol, 92.8%) of methyltris(4-chlorophenyl)phosphonium iodide was obtained: mp>250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837392 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-1c40da71eafb4508bd57caba3036afc4 |
| Source note | uspto-grants-1989_06 |