HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 20039280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Phosphine, tris[3-(trifluoromethyl)phenyl]- | HCID 427977 | — |
| Product | HCID 20039280 | HCID 20039280 | 82.5% |
Reaction Steps
Starting from 2.39 g (5.13 mmol) of tris(3-trifluoromethylphenyl)phosphine and 1.10 g (7.75 mmol, 1.51 eq) of methyl iodide, 2.57 g (4.23 mmol, 82.4%) of methyltris(3-trifluoromethylphenyl)phosphonium iodide was obtained: mp 225.1°-229.3° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837392 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-11e7344157b8416492a76ce8d860f0a9 |
| Source note | uspto-grants-1989_06 |