HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 20039294, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 4-chlorobenzenesulfonate | HCID 1551228 | — |
| Product | HCID 20039294 | HCID 20039294 | 157.7% |
Reaction Steps
A mixture of 11.0 g (41.9 mmol) of triphenylphosphine and 9.16 g (44.4 mmol) of 4-chlorobenzenesulfonate was allowed to react for 2 hr at 140° C. A total of 16.4 g (35.0 mmol, 83.5%) of the title product was obtained. It was further purified by recrystallization from 95:5 toluene-acetonitrile. Analyses: mp 123.2°-125.2° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837392 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-d9880a9d1ceb46beab4b0b5d5444fbcf |
| Source note | uspto-grants-1989_06 |