HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl p-toluenesulfonate → HCID 19831322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | Phosphine, tris(4-methylphenyl)- | HCID 13956 | — |
| Product | HCID 19831322 | HCID 19831322 | 62% |
Reaction Steps
A mixture of 2.38 g (7.82 mmol) of tris(4-methylphenyl)phosphine and 1.53 g (8.22 mmol) of methyl tosylate were allowed to react for 1 hr at 130° C. A total of 2.38 g (4.85 mmol, 62.0%) of product was obtained, which was further purified by recrystallizatin from 97:3 toluene-ethanol. Analyses: mp 103.4°-137.1° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837392 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-e755f4dcf34448e59f43318bbb05408c |
| Source note | uspto-grants-1989_06 |