HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Methyltriphenylphosphonium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Product | Methyltriphenylphosphonium iodide | HCID 638159 | 95.5% |
Reaction Steps
Starting with 10.0 g (38.1 mmol) of triphenylphosphine and 6.8 g (48 mmol, 1.3 eq) of methyl iodide, 14.7 g (36.4 mmol, 95.4%) of methyltriphenylphosphonium iodide was obtained: mp 185.9°-186.8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837391 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-a0390c8ccd194343b4e435a089ac3140 |
| Source note | uspto-grants-1989_06 |