HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 20039285, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Tris(4-trifluoromethylphenyl)phosphine | HCID 139448 | — |
| Product | HCID 20039285 | HCID 20039285 | 89.4% |
Reaction Steps
Starting from 5.01 g (10.7 mmol) of tris (4-trifluoromethylphenyl)phosphine and 3.22 g (22.7 mmol, 2.11 eq) of methyl iodide, 5.82 g (9.57 mmol, 89.4%) of methyltris(4-trifluoromethylphenyl)-phosphonium iodide was obtained: mp>250°;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837391 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-3eab94977efe4269a189a704eee1ad4b |
| Source note | uspto-grants-1989_06 |