HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 20039288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Methyl-4-nitrobenzenesulfonate | HCID 22582 | — |
| Product | HCID 20039288 | HCID 20039288 | 187% |
Reaction Steps
A mixture of 5.83 g (22.2 mmol) of triphenylphosphine and 5.00 g (23.0 mmol) methyl 4-nitrobenzenesulfonate was allowed to react for 2 hrs at 145° C. A total of 10.3 g (21.5 mmol, 96.8%) of the product was obtained, which was further purified by recrystallization from 90:10 toluene-acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837391 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-4b2dc9e4efbc468a93c166b6b04d5240 |
| Source note | uspto-grants-1989_06 |