HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl p-toluenesulfonate → HCID 20039278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | Phosphine, tris(4-methoxyphenyl)- | HCID 70071 | — |
| Product | HCID 20039278 | HCID 20039278 | 73% |
Reaction Steps
A mixture of 5.37 g (15.2 mmol) of tris (4-methoxyphenyl)phosphine and 2.95 G (15.8 mmol) of methyl tosylate was allowed to react for 1 hr at 135° C. A total of 5.96 g (11.1 mmol, 73.0%) of the product was obtained, which was further purified by recrystallization from 97:3 toluene-ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04837391 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-4cd042e653cb4bce8d658c2341e0d6fa |
| Source note | uspto-grants-1989_06 |