Acetic Anhydride → HCID 14576922, compound

Participants

Reaction Conditions

Reaction Steps

To 1.00 g of 1-(4-chlorophenyl)-6-(4-hydroxyphenyl)-2-piperidone was added 25 ml of acetic anhydride and the mixture was stirred at 120° C. for 1 hour. The solvent was evaporated under reduced pressure and the residue was recrystallized from ethyl acetate to give 910 mg of 1-(4-chlorophenyl)-6-(4-acetoxyphenyl)-2-piperidone as colorless prisms.

Provenance & Evidence