HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → HCID 12803111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | HCID 12803100 | HCID 12803100 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12803111 | HCID 12803111 | — |
Reaction Steps
Following the method of Example 4(i), 5-amino-1H-indole-3-acetonitrile (0.8 g) in dimethylformamide (10 ml) was reacted with methyl chloroformate (0.5 ml) to give the title compound (0.44 g) as a white solid m.p. 146°-8° after column chromatography (Kieselgel 60, 100 g) eluted with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04839377 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-e950d3d91b68467d97025fbe55a92fb9 |
| Source note | uspto-grants-1989_06 |