Methanol → HCID 86743081, compound

HRID 1904804Notes

Reaction equation

HRID 1904804 reaction equation
[CH2:1]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[S:19]([OH:22])(=[O:21])=[O:20])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].C(N)(=O)C1OC1.CO.[CH3:31][C:32]1([CH3:37])[NH:36][CH2:35][CH2:34][O:33]1>O>[CH2:1]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[S:19]([OH:22])(=[O:20])=[O:21])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH3:31][C:32]1([CH3:37])[NH:36][CH2:35][CH2:34][O:33]1

Participants

5

Reactant 3

HCID 887MethanolHCID 5506972,2-Dimethyl-oxazolidineHCID 86743080HCID 86743080, compound

Product 1

HCID 86743081HCID 86743081, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

204.0 parts by weight of the 70% dodecylbenzene sulfonic acid solution of Example 3 is mixed with 233.5 grams of additional Methanol. This solution is then added to 62.5 grams of a 78% dimethyloxazolidine solution in water, supplied by Angus Chemicals. These two components are then mixed till clear and homogeneous.

Workup

  1. additionThese two components are then mixed till clear and homogeneous

Sources & evidence

ORD record
ord-44501b5079f14e00ad9bd34b4c99e0a8
Source dataset
uspto-grants-1989_06
Patent number
US04839427

Reaction notes

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