Benzoyl chloride → Benzamide, N-(5-chloro-2-hydroxy-4-nitrophenyl)-

Participants

Reaction Steps

In 100 ml of ethyl acetate was dissolved 40 g (210×10-3 mole) of 2-amino-4-chloro-5-nitrophenol, and 33 g of benzoyl chloride was added at room temperature and then the mixture was refluxed under heating for 2 hours. After the reaction, a solvent was distilled off under reduced pressure and the residue was recrystallized from hexane to obtain products. Yield: 60 g.

Provenance & Evidence