Potassium Hydroxide → HCID 13576835, compound

HRID 1905032Notes

Reaction equation

HRID 1905032 reaction equation
[C:1]([CH:4]1[CH:18]2[CH:7]([CH2:8][C:9]3[C:17]4[C:16]2=[CH:15][CH:14]=[CH:13][C:12]=4[N:11](S(C2C=CC=CC=2)(=O)=O)[CH:10]=3)[N:6]([CH3:28])[CH2:5]1)(=[O:3])[CH3:2].[OH-].[K+]>C(O)C>[C:1]([CH:4]1[CH:18]2[CH:7]([CH2:8][C:9]3[C:17]4[C:16]2=[CH:15][CH:14]=[CH:13][C:12]=4[NH:11][CH:10]=3)[N:6]([CH3:28])[CH2:5]1)(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 13576795HCID 13576795, compound

Product 1

HCID 13576835HCID 13576835, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Debenzenesulphonylation of the 9-acetyl compound (Example 4) (0.20 g) was achieved with potassium hydroxide in refluxing ethanol by the procedure previously described.

Sources & evidence

ORD record
ord-b75c52bcfed34f8899479445ff6919ca
Source dataset
uspto-grants-1989_06
Patent number
US04841056

Reaction notes

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