HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1905323Generated: November 2, 2026
Isoamyl Alcohol → (2RS, 3S)-3-carbobenzoxyamino-2-hydroxy-5-methylhexyl isoamyl ether
https://huagongshe.com/reaction/1905323
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isoamyl Alcohol | HCID 31260 | — |
| Reactant | (3S)-3-carbobenzoxyamino-5-methyl-1,2-epoxyhexane | HCID 13909433 | — |
| Product | (2RS, 3S)-3-carbobenzoxyamino-2-hydroxy-5-methylhexyl isoamyl ether | HCID 131715982 | — |
Reaction Steps
A mixture of 100 mg of (3S)-3-carbobenzoxyamino-5-methyl-1,2-epoxyhexane, 2 g of dry neutral alumina, and 2 ml of isoamyl alcohol was stirred for 16 hours at 100° C., and then stirred for 90 minutes at 140° C. After filtration of the alumina, the filtrate was evaporated under reduced pressure to obtain 97 mg of (2RS, 3S)-3-carbobenzoxyamino-2-hydroxy-5-methylhexyl isoamyl ether as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04841067 |
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| Source dataset | uspto-grants-1989_06 |
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| ORD ID | ord-830317dd1dd1417abb94cfc1abdc8027 |
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| Source note | uspto-grants-1989_06 |
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