Sodium Hydroxide → HCID 86743191, compound

HRID 1905404Notes

Reaction equation

HRID 1905404 reaction equation
[CH3:1][N:2]1[C:6]([O:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[C:5]([CH:14]=[N:15][O:16][CH2:17][C:18]2[CH:26]=[CH:25][C:21]([C:22]([OH:24])=[O:23])=[CH:20][CH:19]=2)[C:4]([CH3:27])=[N:3]1.[OH-].[Na+:29]>O>[CH3:1][N:2]1[C:6]([O:7][C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=2)=[C:5]([CH:14]=[N:15][O:16][CH2:17][C:18]2[CH:19]=[CH:20][C:21]([C:22]([O-:24])=[O:23])=[CH:25][CH:26]=2)[C:4]([CH3:27])=[N:3]1.[Na+:29]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 545462834-[[(Z)-(1,3-Dimethyl-5-phenoxypyrazol-4-yl)methylideneamino]oxymethyl]benzoic acid

Product 1

HCID 86743191HCID 86743191, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

1.0 Gram (0.0027 mole) of 4-[(1,3-dimethyl-5-phenoxypyrazol-4-yl)methyleneaminooxymethyl]benzoic acid and 0.07 g (0.0028 mole) of sodium hydroxide were added to 10 ml of water, and the resulting mixture was stirred for 2 hours. After completion of the reaction, water was removed by evaporation under reduced pressure to obtain the desired compound in a quantitative yield.

Workup

  1. customwas removed by evaporation under reduced pressure

Sources & evidence

ORD record
ord-d5430fa3584346e8809938909ca3b59f
Source dataset
uspto-grants-1989_06
Patent number
US04843068

Reaction notes

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