HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14648884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-(3,4-Dimethoxyphenyl)cyclohexanecarbonitrile | HCID 4639353 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 14648882 | HCID 14648882 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14648884 | HCID 14648884 | — |
Reaction Steps
A solution of 4-(3,4-dimethoxyphenyl)-4-cyanocyclohexane (5 mmol), N-(1-methylethyl)-4-(3,4-dimethoxyphenyl)butylamine hydrochloride (5 mmol), triethylamine (6 mmol) and sodium cyanoborohydride (6 mmol) in 25 ml ethanol was stirred at 25° C. for 72 hours and worked up and recrystallized. ##STR8##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04843081 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-20856a0e1e154a559095ae9c3cf54479 |
| Source note | uspto-grants-1989_06 |