HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitroethane → 2,4-Dimethoxy-1-(2-nitroprop-1-en-1-yl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | 2,4-Dimethoxybenzaldehyde | HCID 69175 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Product | 2,4-Dimethoxy-1-(2-nitroprop-1-en-1-yl)benzene | HCID 600723 | — |
Reaction Steps
A solution consisting of 25 g of 2,4-dimethoxybenzaldehyde (Aldrich) in 200 ml of nitroethane was treated with 0.5 g anhydrous ammonium acetate and held on a steam bath for 12 hours. The solvent was removed in vacuo from the mixture yielding 22.3 g of yellow crystals, m.p. 80°-81° C., upon cooling in 50 ml of methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04647446 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-457ba05c78d94d4da91185c66cc6b672 |
| Source note | uspto-grants-1987_03 |