HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20138883, compound → HCID 13756027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20138883 | HCID 20138883 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13756027 | HCID 13756027 | — |
Reaction Steps
5% Palladium on carbon (3.0 g) is added to a solution of 5-methoxy-1-piperidinylmethyl-1,2-dihydronaphthalene (63 g) in absolute ethanol (600 ml) and placed under H2 at an initial pressure of 47 psi for 30 min. The reaction mixture is filtered and the filtrate evaporated in vacuo yielding the desired product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04647559 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-16305a433fe24a008c1fe03b6ccf6aae |
| Source note | uspto-grants-1987_03 |