HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54206619, compound → HCID 20138914, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54206619 | HCID 54206619 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20138914 | HCID 20138914 | — |
Reaction Steps
A suspension of the 1-cyano compound of Step 1. (53.2 g) and 5% palladium on carbon (5.3 g) in ethanol (530 ml) is stirred under an atmosphere of H2 for four hours. The reaction mixture is filtered, and the filtrate evaporated in vacuo affording the crude product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04647559 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-cbe96eef8489471fad101f0b895e20d0 |
| Source note | uspto-grants-1987_03 |