HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 275570, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 3,4,5-Trimethoxybenzaldehyde | HCID 6858 | — |
| Reactant | Hydantoin | HCID 10006 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 275570 | HCID 275570 | 87% |
Reaction Steps
50 g (0.5 mole) of hydantoine, 98.1 g (0.5 mole) of 3,4,5-trimethoxy-benzaldehyde and 46 g (0.7 mole) of ethanol amine are admixed with 500 ml of water at 70° C. The reaction is carried out further in accordance with Example 2. Thus 121 g of the desired compound are obtained, yield 87%. Mp.: 266°-268° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04647694 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-32cfa3f5c5ef4b52a058eca768124a13 |
| Source note | uspto-grants-1987_03 |