Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | STK017412 | HCID 302666 | — |
| Product | HCID 70426821 | HCID 70426821 | — |
Reaction Steps
To a stirred solution of 19.9 g (0.103 mol) alpha-(2,6-dimethylphenylamino)acethydrazide in 350 ml dichloromethane was added quickly 11.3 g (0.103 mol) acetic anhydride. A mild exotherm ensued. After being stirred at about 25° C. for about 16 hours, the reaction mixture was filtered to give 8.9 g of 1-(2,6-dimethylphenylaminoacetyl)-2-acetyl hydrazine, m.p. 148°-150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04648897 |
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| Source dataset | uspto-grants-1987_03 |
|---|
| ORD ID | ord-3e8b8e04236644d2b34d24044f9c627b |
|---|
| Source note | uspto-grants-1987_03 |
|---|
