Chloroacetic Acid → HCID 13208926, compound

HRID 1905977Notes

Reaction equation

HRID 1905977 reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([CH2:7][CH2:8][OH:9])=[CH:5][CH:4]=1.Cl[CH2:13][C:14]([OH:16])=[O:15]>C1(C)C=CC=CC=1>[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([CH2:7][CH2:8][O:9][CH2:13][C:14]([OH:16])=[O:15])=[CH:5][CH:4]=1

Participants

4

Reactant 2

HCID 300Chloroacetic AcidHCID 697054-Methoxyphenethyl alcohol

Product 1

HCID 13208926HCID 13208926, compoundYield 79.1%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

6.08 g of 4-methoxyphenethyl alcohol were reacted with 3.8 g of chloroacetic acid in a manner analogous to that described in Example 4(a) to give 6.64 g (79%) of 2-(4-methoxyphenyl)ethoxyacetic acid of melting point 82°-84° C. (from toluene).

Sources & evidence

ORD record
ord-5695cea4125a4c1eae8a655e8549678c
Source dataset
uspto-grants-1987_03
Patent number
US04649160

Reaction notes

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