HCID 13208926, compound → HCID 13208933, compound

HRID 1905978Notes

Reaction equation

HRID 1905978 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][O:11][CH2:12][C:13](O)=[O:14])=[CH:5][CH:4]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([CH2:9][CH2:10][O:11][CH2:12][CH2:13][OH:14])=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 13208926HCID 13208926, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 13208933HCID 13208933, compoundYield 96%

Procedure

The 2-(4-methoxyphenyl)ethoxyacetic acid obtained according to the preceding paragraph was reduced with lithium aluminum hydride in a manner analogous to that described in Example 1(b) to give 5.4 g (96%) of 2-[2-(4-methoxyphenyl)ethoxy]ethanol in the form of an oil which was homogeneous according to chromatography.

Sources & evidence

ORD record
ord-e140a0c0a9bf451f87e347600d1531c0
Source dataset
uspto-grants-1987_03
Patent number
US04649160

Reaction notes

Loading…