Citric Acid → HCID 6917927, compound

HRID 1906042Notes

Reaction equation

HRID 1906042 reaction equation
[C:1]([OH:13])(=[O:12])[CH2:2][C:3]([CH2:8][C:9]([OH:11])=[O:10])([C:5]([OH:7])=[O:6])[OH:4].[CH3:14][N:15]1[C@H:19]2[C@H:20]3[N:25]4[C@H:26]([O:27][CH2:28][C@H:24]4[C:23]4[C:29]([O:33][CH3:34])=[CH:30][CH:31]=[CH:32][C:22]=4[CH2:21]3)[C@@H:16]1[CH2:17][C@H:18]2[C:35]([O-:37])=[O:36]>>[CH3:14][N:15]1[CH:19]2[CH:20]3[N:25]4[CH:26]([O:27][CH2:28][CH:24]4[C:23]4[C:29]([O:33][CH3:34])=[CH:30][CH:31]=[CH:32][C:22]=4[CH2:21]3)[CH:16]1[CH2:17][CH:18]2[C:35]([OH:37])=[O:36].[CH2:8]([C:3]([OH:4])([C:5]([OH:7])=[O:6])[CH2:2][C:1]([OH:13])=[O:12])[C:9]([OH:11])=[O:10]

Participants

3

Reactant 2

HCID 311Citric AcidHCID 91820461HCID 91820461, compound

Product 1

HCID 6917927HCID 6917927, compound

Procedure

In this example, 10 ml of the DC-52 millipore filtrate obtained in Example 1 is cooled to 5° C., adjusted to pH 3.0 with citric acid, and then freeze-dried to obtain 630 mg of DC-52 citrate powder (equivalent weight ratio: 1.1).

Workup

  1. customis cooled to 5° C.
  2. customfreeze-dried

Sources & evidence

ORD record
ord-2130f878c0614dfab7f07c92ca76cc0e
Source dataset
uspto-grants-1987_03
Patent number
US04649199

Reaction notes

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