HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Epoxyeicosane → 3-(2-Hydroxyeicosyloxy)-2-methoxypropyl tetrahydropyranyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Epoxyeicosane | HCID 89221 | — |
| Reactant | 2-Methylglycerol tetrahydropyranyl ether | HCID 13563077 | — |
| Product | 3-(2-Hydroxyeicosyloxy)-2-methoxypropyl tetrahydropyranyl ether | HCID 20213827 | 58.7% |
Reaction Steps
The above epoxide (17) (4.75 g, 16 mmoles) was reacted with 6.1 g (32 mmoles) of 2-methylglycerol monotetrahydropyranyl ether in the same manner as Example 1-2 to give 4.57 g of the desired compound as a colorless wax.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04649203 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-88de6ce2256f447a9242dc7ac211e729 |
| Source note | uspto-grants-1987_03 |