関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | N-(hydroxymethyl)benzamide | HCID 80493 | — |
| 反応物 | 2-(4-Chlorophenyl)-6-methylimidazo[1,2-a]pyridine | HCID 735911 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | 2-(4-Chlorophenyl)-3-benzoylaminomethyl-6-methylimidazo[1,2-a]pyridine | HCID 13589589 | — |
反応手順
To a solution of 4.54 g (0.03 mol) of N-(hydroxymethyl)benzamide in 50 ml of glacial acetic acid, 2 g of concentrated sulphuric acid are added, and then, after 15 minutes' heating at 50° C., 4.8 g (0.02 mol) of 2-(4-chlorophenyl)-6-methylimidazo[1,2-a]pyridine are added.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04650796 |
|---|
| 出典データセット | uspto-grants-1987_03 |
|---|
| ORD ID | ord-f09ddaa63a2d4d9f960d9774a8536c03 |
|---|
| 出典メモ | uspto-grants-1987_03 |
|---|
