HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobutanal → HCID 20212854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobutanal | HCID 242200 | — |
| Reactant | HCID 20212863 | HCID 20212863 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20212854 | HCID 20212854 | — |
Reaction Steps
A mixture of 4-chlorobutanal (1.8 g) and 2-(4-hydrazinophenyl)acetamide hydrochloride (3 g) in 50% aqueous acetic acid (200 ml) was heated at reflux for 45 min., then cooled and evaporated to give 3-(2-chloroethyl)-1H-indole-5-acetamide as a dark organe-brown foam. τ (DMSO) 6.3(2H); 6,8(2H); (CH2CH2Cl)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04650810 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-cc9ff39187e24b14b341abea70aff897 |
| Source note | uspto-grants-1987_03 |