Diethylethanolamine → HCID 11403412, compound

Participants

Reaction Conditions

Reaction Steps

140.6 grams (1.2 moles) of diethyl ethanolamine, 48 grams (1.2 moles) of sodium hydroxide and 288.4 grams (1 mole) of lauryl sulfate, Na salt were reacted under a nitrogen atmosphere using the procedure of Example 9. Approx. 20 grams of the diethyl ethanolamine evaporated from the reaction with water during the reaction and was immediately replaced. After a reaction time of 2 hours at 190° C., followed by cooling to 20° C., the reaction mixture was purified using the procedure of Example 2. 168 grams of an oily liquid having an amine number of 151 were obtained.

Provenance & Evidence