Triethylamine → HCID 13823416, compound

Participants

Reaction Steps

A mixture of 0.85 g (0.004 mole) 3-n-butyl-2-mercapto-4(3H)-quinazolinone (the product of Example 6), 1.54 g (0.004 mole) chlorotriphenyl tin and 0.4 g (0.004 mole) triethylamine in methylene chloride (about 100 ml) was stirred for one hour, refluxed 5.5 hours, stirred overnight and refluxed 8 hours. The reaction mixture was washed with water. The organic phase was dried over magnesium sulfate, and stripped to obtain the above-identified product as a solid, melting point 112° to 114° C.

Provenance & Evidence